The preparation and preliminary characterisation of eight geological MPI-DING reference glasses for in-situ microanalysis

Research output: Contribution to journalArticleResearchpeer review

Authors

  • Klaus Peter Jochum
  • Donald B. Dingwell
  • Alexander Rocholl
  • Brigitte Stoll
  • Albrecht W. Hofmann
  • S. Becker
  • A. Besmehn
  • D. Besserte
  • H. J. Dietze
  • P. Dulski
  • J. Erzinger
  • E. Hellebrand
  • P. Hoppe
  • I. Horn
  • K. Janssens
  • G. A. Jenner
  • M. Klein
  • W. F. McDonough
  • M. Maetz
  • K. Mezger
  • C. Münker
  • I. K. Nikogosian
  • C. Pickhardt
  • I. Raczek
  • D. Rhede
  • H. M. Seufert
  • S. G. Simakin
  • A. V. Sobolev
  • B. Spettel
  • S. Straub
  • L. Vincze
  • A. Wallianos
  • G. Weckwerth
  • S. Weyer
  • D. Wolf
  • M. Zimmer

External Research Organisations

  • Max Planck Institute for Chemistry (Otto Hahn Institute)
  • University of Bayreuth
  • Heidelberg University
  • Helmholtz Centre Potsdam - German Research Centre for Geosciences (GFZ)
  • Forschungszentrum Jülich
  • Universität Hamburg
  • Harvard University
  • University of Antwerp (UAntwerpen)
  • Memorial University of Newfoundland
  • University of Cologne
  • Max Planck Institute for Nuclear Physics
  • University of Münster
  • Vrije Universiteit
  • RAS - Institute of Microelectronics and Informatics
  • Russian Academy of Sciences (RAS)
  • GEOMAR Helmholtz Centre for Ocean Research Kiel
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Details

Original languageEnglish
Pages (from-to)87-133
Number of pages47
JournalGeostandards Newsletter
Volume24
Issue number1
Publication statusPublished - 2000
Externally publishedYes

Abstract

Eight silicate glasses were prepared by directly fusing and stirring 50-100 g each of basalt, andesite, komatiite, peridotite, rhyolite, and quartz-diorite. These are referred to as MPI-DING glasses and were made for the purpose of providing reference materials for geochemical, in-situ microanalytical work. Results from various analytical techniques indicate that individual glass fragments are well homogenised with respect to major and trace elements at the μm to mm scale. Heterogeneities due to quench crystallisation of olivine have been observed in small and limited areas of the two komatiitic glasses. In order to obtain concentration values for as many elements as possible, the glasses were analysed by a variety of bulk and microanalytical methods in a number of laboratories. From the analytical data, preliminary reference values for more than sixty elements were calculated. The analytical uncertainties of most elements are estimated to be between 1% and 10%.

Keywords

    Characterisation, Geological glasses, In-situ techniques, Microprobe analysis, Preparation, Reference materials

ASJC Scopus subject areas

Cite this

The preparation and preliminary characterisation of eight geological MPI-DING reference glasses for in-situ microanalysis. / Jochum, Klaus Peter; Dingwell, Donald B.; Rocholl, Alexander et al.
In: Geostandards Newsletter, Vol. 24, No. 1, 2000, p. 87-133.

Research output: Contribution to journalArticleResearchpeer review

Jochum, KP, Dingwell, DB, Rocholl, A, Stoll, B, Hofmann, AW, Becker, S, Besmehn, A, Besserte, D, Dietze, HJ, Dulski, P, Erzinger, J, Hellebrand, E, Hoppe, P, Horn, I, Janssens, K, Jenner, GA, Klein, M, McDonough, WF, Maetz, M, Mezger, K, Münker, C, Nikogosian, IK, Pickhardt, C, Raczek, I, Rhede, D, Seufert, HM, Simakin, SG, Sobolev, AV, Spettel, B, Straub, S, Vincze, L, Wallianos, A, Weckwerth, G, Weyer, S, Wolf, D & Zimmer, M 2000, 'The preparation and preliminary characterisation of eight geological MPI-DING reference glasses for in-situ microanalysis', Geostandards Newsletter, vol. 24, no. 1, pp. 87-133. https://doi.org/10.1111/j.1751-908X.2000.tb00590.x
Jochum, K. P., Dingwell, D. B., Rocholl, A., Stoll, B., Hofmann, A. W., Becker, S., Besmehn, A., Besserte, D., Dietze, H. J., Dulski, P., Erzinger, J., Hellebrand, E., Hoppe, P., Horn, I., Janssens, K., Jenner, G. A., Klein, M., McDonough, W. F., Maetz, M., ... Zimmer, M. (2000). The preparation and preliminary characterisation of eight geological MPI-DING reference glasses for in-situ microanalysis. Geostandards Newsletter, 24(1), 87-133. https://doi.org/10.1111/j.1751-908X.2000.tb00590.x
Jochum KP, Dingwell DB, Rocholl A, Stoll B, Hofmann AW, Becker S et al. The preparation and preliminary characterisation of eight geological MPI-DING reference glasses for in-situ microanalysis. Geostandards Newsletter. 2000;24(1):87-133. doi: 10.1111/j.1751-908X.2000.tb00590.x
Jochum, Klaus Peter ; Dingwell, Donald B. ; Rocholl, Alexander et al. / The preparation and preliminary characterisation of eight geological MPI-DING reference glasses for in-situ microanalysis. In: Geostandards Newsletter. 2000 ; Vol. 24, No. 1. pp. 87-133.
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abstract = "Eight silicate glasses were prepared by directly fusing and stirring 50-100 g each of basalt, andesite, komatiite, peridotite, rhyolite, and quartz-diorite. These are referred to as MPI-DING glasses and were made for the purpose of providing reference materials for geochemical, in-situ microanalytical work. Results from various analytical techniques indicate that individual glass fragments are well homogenised with respect to major and trace elements at the μm to mm scale. Heterogeneities due to quench crystallisation of olivine have been observed in small and limited areas of the two komatiitic glasses. In order to obtain concentration values for as many elements as possible, the glasses were analysed by a variety of bulk and microanalytical methods in a number of laboratories. From the analytical data, preliminary reference values for more than sixty elements were calculated. The analytical uncertainties of most elements are estimated to be between 1% and 10%.",
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AU - Jochum, Klaus Peter

AU - Dingwell, Donald B.

AU - Rocholl, Alexander

AU - Stoll, Brigitte

AU - Hofmann, Albrecht W.

AU - Becker, S.

AU - Besmehn, A.

AU - Besserte, D.

AU - Dietze, H. J.

AU - Dulski, P.

AU - Erzinger, J.

AU - Hellebrand, E.

AU - Hoppe, P.

AU - Horn, I.

AU - Janssens, K.

AU - Jenner, G. A.

AU - Klein, M.

AU - McDonough, W. F.

AU - Maetz, M.

AU - Mezger, K.

AU - Münker, C.

AU - Nikogosian, I. K.

AU - Pickhardt, C.

AU - Raczek, I.

AU - Rhede, D.

AU - Seufert, H. M.

AU - Simakin, S. G.

AU - Sobolev, A. V.

AU - Spettel, B.

AU - Straub, S.

AU - Vincze, L.

AU - Wallianos, A.

AU - Weckwerth, G.

AU - Weyer, S.

AU - Wolf, D.

AU - Zimmer, M.

PY - 2000

Y1 - 2000

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KW - Geological glasses

KW - In-situ techniques

KW - Microprobe analysis

KW - Preparation

KW - Reference materials

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VL - 24

SP - 87

EP - 133

JO - Geostandards Newsletter

JF - Geostandards Newsletter

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IS - 1

ER -

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