Details
| Original language | English |
|---|---|
| Pages (from-to) | 3741-3744 |
| Number of pages | 4 |
| Journal | ORGANOMETALLICS |
| Volume | 23 |
| Issue number | 15 |
| Publication status | Published - 17 Jun 2004 |
Abstract
The synthesis of substituted arene molybdenum complexes via arene exchange was investigated. All manipulations with Mo complexes were carried out under an atmosphere of purified nitrogen using standard inert gas/vacuum double manifold and Schlenk techniques. The reaction time was shortened by reacting Mo(CO) 6 in benzene in the presence of pyridine in an autoclave. The synthesis of the molybdenum complexes via arene exchange reaction results in higher yields, shorter reaction times, and easy workup.
ASJC Scopus subject areas
- Chemistry(all)
- Physical and Theoretical Chemistry
- Chemistry(all)
- Organic Chemistry
- Chemistry(all)
- Inorganic Chemistry
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In: ORGANOMETALLICS, Vol. 23, No. 15, 17.06.2004, p. 3741-3744.
Research output: Contribution to journal › Article › Research › peer review
}
TY - JOUR
T1 - Synthesis of substituted arene molybdenum complexes by arene exchange
AU - Kündig, E. Peter
AU - Fabritius, Charles Henry
AU - Grossheimann, Gabriele
AU - Romanens, Patrick
AU - Butenschön, Holger
AU - Wey, Hans Günther
PY - 2004/6/17
Y1 - 2004/6/17
N2 - The synthesis of substituted arene molybdenum complexes via arene exchange was investigated. All manipulations with Mo complexes were carried out under an atmosphere of purified nitrogen using standard inert gas/vacuum double manifold and Schlenk techniques. The reaction time was shortened by reacting Mo(CO) 6 in benzene in the presence of pyridine in an autoclave. The synthesis of the molybdenum complexes via arene exchange reaction results in higher yields, shorter reaction times, and easy workup.
AB - The synthesis of substituted arene molybdenum complexes via arene exchange was investigated. All manipulations with Mo complexes were carried out under an atmosphere of purified nitrogen using standard inert gas/vacuum double manifold and Schlenk techniques. The reaction time was shortened by reacting Mo(CO) 6 in benzene in the presence of pyridine in an autoclave. The synthesis of the molybdenum complexes via arene exchange reaction results in higher yields, shorter reaction times, and easy workup.
UR - http://www.scopus.com/inward/record.url?scp=3342985036&partnerID=8YFLogxK
U2 - 10.1021/om049792m
DO - 10.1021/om049792m
M3 - Article
AN - SCOPUS:3342985036
VL - 23
SP - 3741
EP - 3744
JO - ORGANOMETALLICS
JF - ORGANOMETALLICS
SN - 0276-7333
IS - 15
ER -