Solid-phase-assisted solution-phase synthesis with minimum purification - Preparation of 2-deoxyglycoconjugates from thioglycosides

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  • Clausthal University of Technology
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Translated title of the contributionEine neue Klasse potenzieller aromatischer Verbindungen: die metallzentrierten planaren Kationen [Fe(Sb5)]+ und [Fe(Bi5)]
Original languageEnglish
Pages (from-to)1166-1170
Number of pages5
JournalAngewandte Chemie
Volume42
Issue number10
Publication statusPublished - 10 Mar 2003

Abstract

Minimum effort - maximum effect: Deoxygenated oligosaccharides and glycoconjugates are prepared in high yields with minimum purification from thioglycosides (see scheme) by exclusively employing reagents that are removed by simple filtration. New solidphase-assisted synthetic protocols for removal of thiophenol and diphenyl disulfide are disclosed that make use of functionalized polymers. RO=testosteryl.

Keywords

    Functionalized polymers, Glycosidation, Separation techniques, Solid-phase synthesis, Thioglycosides

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Solid-phase-assisted solution-phase synthesis with minimum purification - Preparation of 2-deoxyglycoconjugates from thioglycosides. / Jaunzems, Janis; Hofer, Edgar; Jesberger, Martin et al.
In: Angewandte Chemie , Vol. 42, No. 10, 10.03.2003, p. 1166-1170.

Research output: Contribution to journalArticleResearchpeer review

Jaunzems J, Hofer E, Jesberger M, Sourkouni-Argirusi G, Kirschning A. Solid-phase-assisted solution-phase synthesis with minimum purification - Preparation of 2-deoxyglycoconjugates from thioglycosides. Angewandte Chemie . 2003 Mar 10;42(10):1166-1170. doi: 10.1002/anie.200390307, 10.1002/ange.200390307
Jaunzems, Janis ; Hofer, Edgar ; Jesberger, Martin et al. / Solid-phase-assisted solution-phase synthesis with minimum purification - Preparation of 2-deoxyglycoconjugates from thioglycosides. In: Angewandte Chemie . 2003 ; Vol. 42, No. 10. pp. 1166-1170.
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AU - Jaunzems, Janis

AU - Hofer, Edgar

AU - Jesberger, Martin

AU - Sourkouni-Argirusi, Georgia

AU - Kirschning, Andreas

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KW - Functionalized polymers

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KW - Separation techniques

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