Details
| Original language | English |
|---|---|
| Pages (from-to) | 295-297 |
| Number of pages | 3 |
| Journal | Journal of Organic Chemistry |
| Volume | 73 |
| Issue number | 1 |
| Publication status | Published - 7 Dec 2007 |
Abstract
(Chemical Equation Presented) Preparation, structural characterization, and reactivity of 3-[bis(trifluoroacetoxy)iodo]benzoic acid and 3-[hydroxy-(tosyloxy)iodo]benzoic acid, new recyclable iodine(III) reagents derived from 3-iodosylbenzoic acid, are described. The reduced form of these reagents, 3-iodobenzoic acid, can be easily recovered from the reaction mixtures using ion-exchange resin or basic aqueous workup followed by acidification with HCl.
ASJC Scopus subject areas
- Chemistry(all)
- Organic Chemistry
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In: Journal of Organic Chemistry, Vol. 73, No. 1, 07.12.2007, p. 295-297.
Research output: Contribution to journal › Article › Research › peer review
}
TY - JOUR
T1 - Preparation and X-ray structures of 3-[bis(trifluoroacetoxy)iodo]benzoic acid and 3-[hydroxy(tosyloxy)iodo]benzoic acid
T2 - New recyclable hypervalent iodine reagents
AU - Yusubov, Mekhman S.
AU - Funk, Tatyana V.
AU - Chi, Ki Whan
AU - Cha, Eun Hye
AU - Ghyung, Hwa Kim
AU - Kirschning, Andreas
AU - Zhdankin, Viktor V.
PY - 2007/12/7
Y1 - 2007/12/7
N2 - (Chemical Equation Presented) Preparation, structural characterization, and reactivity of 3-[bis(trifluoroacetoxy)iodo]benzoic acid and 3-[hydroxy-(tosyloxy)iodo]benzoic acid, new recyclable iodine(III) reagents derived from 3-iodosylbenzoic acid, are described. The reduced form of these reagents, 3-iodobenzoic acid, can be easily recovered from the reaction mixtures using ion-exchange resin or basic aqueous workup followed by acidification with HCl.
AB - (Chemical Equation Presented) Preparation, structural characterization, and reactivity of 3-[bis(trifluoroacetoxy)iodo]benzoic acid and 3-[hydroxy-(tosyloxy)iodo]benzoic acid, new recyclable iodine(III) reagents derived from 3-iodosylbenzoic acid, are described. The reduced form of these reagents, 3-iodobenzoic acid, can be easily recovered from the reaction mixtures using ion-exchange resin or basic aqueous workup followed by acidification with HCl.
UR - http://www.scopus.com/inward/record.url?scp=37549064645&partnerID=8YFLogxK
U2 - 10.1021/jo702112s
DO - 10.1021/jo702112s
M3 - Article
C2 - 18062703
AN - SCOPUS:37549064645
VL - 73
SP - 295
EP - 297
JO - Journal of Organic Chemistry
JF - Journal of Organic Chemistry
SN - 0022-3263
IS - 1
ER -