PBF-LB/M process under a silane-doped argon atmosphere: Preliminary studies and development of an innovative machine concept

Research output: Contribution to journalArticleResearchpeer review

Authors

  • Nicole Emminghaus
  • Sebastian Fritsch
  • Hannes Büttner
  • Jannes August
  • Marijan Tegtmeier
  • Michael Huse
  • Marius Lammers
  • Christian Hoff
  • Jörg Hermsdorf
  • Stefan Kaierle

External Research Organisations

  • Laser Zentrum Hannover e.V. (LZH)
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Details

Original languageEnglish
Article number100040
JournalAdvances in Industrial and Manufacturing Engineering
Volume2
Early online date4 Apr 2021
Publication statusPublished - May 2021
Externally publishedYes

Abstract

In laser-based powder bed fusion of metals (PBF-LB/M) the presence of oxygen is known to encourage embrittlement and impair the wetting properties of the substrate and solidified material. Conventionally, inert gases like argon are used to reduce the residual oxygen content within the processing atmosphere. However, especially in terms of reactive materials like titanium the remaining oxygen still causes critical oxidations. In this publication, a new approach for obtaining an oxygen-free processing atmosphere is presented. Thereby the argon shielding gas is doped with reactive monosilane to reduce the residual oxygen content to a range comparable to XHV (Extreme High Vacuum, thermodynamic oxygen activity <10−15). The handling of this new silane-containing atmosphere requires the development of a special manufacturing system. Therefore, this work elucidates the development of an innovative machine system in accordance with the VDI (German Association of Engineers) Guideline 2221. For determination and specification of the underlying requirements, the interaction of the gas mixture with various construction materials and Ti–6Al–4V powder material was investigated in a test chamber. It could be shown that metallic materials and smooth surfaces are favorable for the design while polymers are likely to degrade in silane-containing atmosphere. Further, the design of the gas flow in the build chamber was optimized using flow simulation. In order to avoid the deposition of reaction products in the process zone, a laminar flow should be established, which can be achieved by baffles and honeycomb structures.

Keywords

    Additive manufacturing, Design methodology, Flow simulation, Gas flow, Laser-based powder bed fusion, Monosilane

ASJC Scopus subject areas

Cite this

PBF-LB/M process under a silane-doped argon atmosphere: Preliminary studies and development of an innovative machine concept. / Emminghaus, Nicole; Fritsch, Sebastian; Büttner, Hannes et al.
In: Advances in Industrial and Manufacturing Engineering, Vol. 2, 100040, 05.2021.

Research output: Contribution to journalArticleResearchpeer review

Emminghaus, N, Fritsch, S, Büttner, H, August, J, Tegtmeier, M, Huse, M, Lammers, M, Hoff, C, Hermsdorf, J & Kaierle, S 2021, 'PBF-LB/M process under a silane-doped argon atmosphere: Preliminary studies and development of an innovative machine concept', Advances in Industrial and Manufacturing Engineering, vol. 2, 100040. https://doi.org/10.1016/j.aime.2021.100040
Emminghaus, N., Fritsch, S., Büttner, H., August, J., Tegtmeier, M., Huse, M., Lammers, M., Hoff, C., Hermsdorf, J., & Kaierle, S. (2021). PBF-LB/M process under a silane-doped argon atmosphere: Preliminary studies and development of an innovative machine concept. Advances in Industrial and Manufacturing Engineering, 2, Article 100040. https://doi.org/10.1016/j.aime.2021.100040
Emminghaus N, Fritsch S, Büttner H, August J, Tegtmeier M, Huse M et al. PBF-LB/M process under a silane-doped argon atmosphere: Preliminary studies and development of an innovative machine concept. Advances in Industrial and Manufacturing Engineering. 2021 May;2:100040. Epub 2021 Apr 4. doi: 10.1016/j.aime.2021.100040
Emminghaus, Nicole ; Fritsch, Sebastian ; Büttner, Hannes et al. / PBF-LB/M process under a silane-doped argon atmosphere : Preliminary studies and development of an innovative machine concept. In: Advances in Industrial and Manufacturing Engineering. 2021 ; Vol. 2.
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abstract = "In laser-based powder bed fusion of metals (PBF-LB/M) the presence of oxygen is known to encourage embrittlement and impair the wetting properties of the substrate and solidified material. Conventionally, inert gases like argon are used to reduce the residual oxygen content within the processing atmosphere. However, especially in terms of reactive materials like titanium the remaining oxygen still causes critical oxidations. In this publication, a new approach for obtaining an oxygen-free processing atmosphere is presented. Thereby the argon shielding gas is doped with reactive monosilane to reduce the residual oxygen content to a range comparable to XHV (Extreme High Vacuum, thermodynamic oxygen activity <10−15). The handling of this new silane-containing atmosphere requires the development of a special manufacturing system. Therefore, this work elucidates the development of an innovative machine system in accordance with the VDI (German Association of Engineers) Guideline 2221. For determination and specification of the underlying requirements, the interaction of the gas mixture with various construction materials and Ti–6Al–4V powder material was investigated in a test chamber. It could be shown that metallic materials and smooth surfaces are favorable for the design while polymers are likely to degrade in silane-containing atmosphere. Further, the design of the gas flow in the build chamber was optimized using flow simulation. In order to avoid the deposition of reaction products in the process zone, a laminar flow should be established, which can be achieved by baffles and honeycomb structures.",
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T2 - Preliminary studies and development of an innovative machine concept

AU - Emminghaus, Nicole

AU - Fritsch, Sebastian

AU - Büttner, Hannes

AU - August, Jannes

AU - Tegtmeier, Marijan

AU - Huse, Michael

AU - Lammers, Marius

AU - Hoff, Christian

AU - Hermsdorf, Jörg

AU - Kaierle, Stefan

N1 - Funding Information: Funded by the Deutsche Forschungsgemeinschaft (DFG , German Research Foundation) – Project-ID 394563137 – SFB 1368 .

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