Details
| Original language | English |
|---|---|
| Pages (from-to) | 1699-1702 |
| Number of pages | 4 |
| Journal | Synlett |
| Issue number | 10 |
| Publication status | Published - 15 Jul 2004 |
Abstract
The preparation of a solid Pd(II)-precatalyst and its use in microwave-assisted Suzuki-Miyaura reactions in water is described. The precatalyst is obtained by treatment of 4-pyridine-aldoxime with Na 2PdCl4 and is insoluble in organic solvents as well as in water. Its robustness under microwave conditions and its insolubility allows simple reuse in 'teabags'.
Keywords
- Precatalyst, Pyridine-aldoxime Pd-catalyst, Suzuki-miyaura reactions
ASJC Scopus subject areas
- Chemistry(all)
- Organic Chemistry
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In: Synlett, No. 10, 15.07.2004, p. 1699-1702.
Research output: Contribution to journal › Article › Research › peer review
}
TY - JOUR
T1 - Microwave-assisted Suzuki-Miyaura reactions with an insoluble pyridine-aldoxime Pd-catalyst
AU - Solodenko, Wladimir
AU - Schön, Uwe
AU - Messinger, Josef
AU - Glinschert, Anja
AU - Kirschning, Andreas
PY - 2004/7/15
Y1 - 2004/7/15
N2 - The preparation of a solid Pd(II)-precatalyst and its use in microwave-assisted Suzuki-Miyaura reactions in water is described. The precatalyst is obtained by treatment of 4-pyridine-aldoxime with Na 2PdCl4 and is insoluble in organic solvents as well as in water. Its robustness under microwave conditions and its insolubility allows simple reuse in 'teabags'.
AB - The preparation of a solid Pd(II)-precatalyst and its use in microwave-assisted Suzuki-Miyaura reactions in water is described. The precatalyst is obtained by treatment of 4-pyridine-aldoxime with Na 2PdCl4 and is insoluble in organic solvents as well as in water. Its robustness under microwave conditions and its insolubility allows simple reuse in 'teabags'.
KW - Precatalyst
KW - Pyridine-aldoxime Pd-catalyst
KW - Suzuki-miyaura reactions
UR - http://www.scopus.com/inward/record.url?scp=4143081487&partnerID=8YFLogxK
U2 - 10.1055/s-2004-829546
DO - 10.1055/s-2004-829546
M3 - Article
AN - SCOPUS:4143081487
SP - 1699
EP - 1702
JO - Synlett
JF - Synlett
SN - 0936-5214
IS - 10
ER -