Individualized and controlled laser beam pre-treatment process for adhesive bonding of fiber-reinforced plastics. III. Effects of contaminants

Research output: Contribution to journalArticleResearchpeer review

Authors

  • Hagen Dittmar
  • Christoph J.A. Beier
  • Josef Weiland
  • Alexander Schiebahn
  • Peter Jaeschke
  • Stefan Kaierle
  • Uwe Reisgen
  • Ludger Overmeyer

External Research Organisations

  • Laser Zentrum Hannover e.V. (LZH)
  • RWTH Aachen University
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Details

Original languageEnglish
Article number042051
Number of pages6
JournalJournal of laser applications
Volume33
Issue number4
Early online date11 Nov 2021
Publication statusPublished - Nov 2021
Externally publishedYes

Abstract

Adhesive bonding of plastic components is a well-established process for various applications. Specifically for thermoplastic parts, surface pre-treatment is required to achieve optimum bonding quality. However, automated surface pre-treatment is not established yet. Reasons are missing process monitoring and significant challenges arising from conventional monitoring techniques that hardly identify surface contaminants. In a recent research project, the authors investigated how process monitoring by spectrometry during a laser-based surface pre-treatment might solve this challenge for fiber-reinforced plastics and generic surface contaminants. This article describes experiments conducted on two composite materials with different contaminants. A nanosecond-pulsed UV-laser was used to pretreat a glass-fiber reinforced 2C-polyurethane (GF-PUR) and a glass-fiber reinforced polyamide 6 (GF-PA6). Each composite had coupons contaminated with an industry standard mould release agent or artificial silicate-based dust as well as uncontaminated samples. The samples were laser pretreated and compared to reference coupons that did not receive laser treatment. The samples were analyzed after laser pre-treatment for their free surface energies by the detection of the contact angle and measured for the surface roughness. The bonding improvement due to the laser process was determined by shear strength and peel resistance tests. The results show that UV-laser pre-treatment has an advantageous impact on the bonding strength of GF-PUR and GF-PA6. Combined with a fast spectrometric process monitoring that robustly identifies contaminants during the laser process, an inline process control is feasible.

ASJC Scopus subject areas

Cite this

Individualized and controlled laser beam pre-treatment process for adhesive bonding of fiber-reinforced plastics. III. Effects of contaminants. / Dittmar, Hagen; Beier, Christoph J.A.; Weiland, Josef et al.
In: Journal of laser applications, Vol. 33, No. 4, 042051, 11.2021.

Research output: Contribution to journalArticleResearchpeer review

Dittmar, H, Beier, CJA, Weiland, J, Schiebahn, A, Jaeschke, P, Kaierle, S, Reisgen, U & Overmeyer, L 2021, 'Individualized and controlled laser beam pre-treatment process for adhesive bonding of fiber-reinforced plastics. III. Effects of contaminants', Journal of laser applications, vol. 33, no. 4, 042051. https://doi.org/10.2351/7.0000466
Dittmar, H., Beier, C. J. A., Weiland, J., Schiebahn, A., Jaeschke, P., Kaierle, S., Reisgen, U., & Overmeyer, L. (2021). Individualized and controlled laser beam pre-treatment process for adhesive bonding of fiber-reinforced plastics. III. Effects of contaminants. Journal of laser applications, 33(4), Article 042051. https://doi.org/10.2351/7.0000466
Dittmar H, Beier CJA, Weiland J, Schiebahn A, Jaeschke P, Kaierle S et al. Individualized and controlled laser beam pre-treatment process for adhesive bonding of fiber-reinforced plastics. III. Effects of contaminants. Journal of laser applications. 2021 Nov;33(4):042051. Epub 2021 Nov 11. doi: 10.2351/7.0000466
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title = "Individualized and controlled laser beam pre-treatment process for adhesive bonding of fiber-reinforced plastics. III. Effects of contaminants",
abstract = "Adhesive bonding of plastic components is a well-established process for various applications. Specifically for thermoplastic parts, surface pre-treatment is required to achieve optimum bonding quality. However, automated surface pre-treatment is not established yet. Reasons are missing process monitoring and significant challenges arising from conventional monitoring techniques that hardly identify surface contaminants. In a recent research project, the authors investigated how process monitoring by spectrometry during a laser-based surface pre-treatment might solve this challenge for fiber-reinforced plastics and generic surface contaminants. This article describes experiments conducted on two composite materials with different contaminants. A nanosecond-pulsed UV-laser was used to pretreat a glass-fiber reinforced 2C-polyurethane (GF-PUR) and a glass-fiber reinforced polyamide 6 (GF-PA6). Each composite had coupons contaminated with an industry standard mould release agent or artificial silicate-based dust as well as uncontaminated samples. The samples were laser pretreated and compared to reference coupons that did not receive laser treatment. The samples were analyzed after laser pre-treatment for their free surface energies by the detection of the contact angle and measured for the surface roughness. The bonding improvement due to the laser process was determined by shear strength and peel resistance tests. The results show that UV-laser pre-treatment has an advantageous impact on the bonding strength of GF-PUR and GF-PA6. Combined with a fast spectrometric process monitoring that robustly identifies contaminants during the laser process, an inline process control is feasible.",
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note = "Funding Information: The authors disclosed receipt of the following financial support for the research, authorship, and/or publication of this article: The IGF-project 19727, “Prozessbeobachtung und -regelung der Klebvorbereitung PUR-und thermoplastbasierter, faserverst{\"a}rkter Kunststoffe mittels Laser—ProKleb” of the research association “DVS German Welding Society” was funded within the framework of the industrial collective research program (IGF) by the Federal Ministry for Economic Affairs and Energy on the basis of a decision by the German Bundestag. The authors would like to express their gratitude toward Coherent, Inc. and C. Meyer for providing the AVIA NX used in the experiments. They also thank T. Engels at Henkel AG & Co. KGaA for providing the materials and O. Lischtschenko at Ocean Optics BV for his continuous support with regard to spectrometry.",
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AU - Dittmar, Hagen

AU - Beier, Christoph J.A.

AU - Weiland, Josef

AU - Schiebahn, Alexander

AU - Jaeschke, Peter

AU - Kaierle, Stefan

AU - Reisgen, Uwe

AU - Overmeyer, Ludger

N1 - Funding Information: The authors disclosed receipt of the following financial support for the research, authorship, and/or publication of this article: The IGF-project 19727, “Prozessbeobachtung und -regelung der Klebvorbereitung PUR-und thermoplastbasierter, faserverstärkter Kunststoffe mittels Laser—ProKleb” of the research association “DVS German Welding Society” was funded within the framework of the industrial collective research program (IGF) by the Federal Ministry for Economic Affairs and Energy on the basis of a decision by the German Bundestag. The authors would like to express their gratitude toward Coherent, Inc. and C. Meyer for providing the AVIA NX used in the experiments. They also thank T. Engels at Henkel AG & Co. KGaA for providing the materials and O. Lischtschenko at Ocean Optics BV for his continuous support with regard to spectrometry.

PY - 2021/11

Y1 - 2021/11

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