Homogeneous annealing of TiO2, ZrO2 and ITO sol-gel layers with CO2 laser

Research output: Contribution to journalConference articleResearchpeer review

Authors

  • M. Desens
  • K. Wesang
  • A. Hohnholz
  • P. Jäschke
  • S. Kaierle
  • L. Overmeyer

External Research Organisations

  • Laser Zentrum Hannover e.V. (LZH)
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Details

Original languageEnglish
Pages (from-to)905-909
Number of pages5
JournalProcedia CIRP
Volume94
Early online date15 Sept 2020
Publication statusPublished - 2020
Externally publishedYes
Event11th CIRP Conference on Photonic Technologies, LANE 2020 - Virtual, Online
Duration: 7 Sept 202010 Sept 2020

Abstract

Laser annealed sol-gel layers have the potential to replace the furnace process and expand the field of applications for selective annealed sol-gel coatings. In this study laser annealed TiO2, ZrO2 and ITO layers on glasses are investigated. Processing parameters of the CO2-laser system such as scanning speed, line overlap, laser power and focal spot are evaluated to generate sufficient thermal energy for densification. The ITO annealing process results in a sheet resistance comparable with the furnace annealed samples. Microscope images of the TiO2 and ZrO2 samples show a homogeneous layer morphology. XRD images exhibit crystalline tetragonal ZrO2 as seen in thermally annealed layers.

Keywords

    ITO, Laser annealing sol gel coating, Surface functionalization, TiO2, ZrO2

ASJC Scopus subject areas

Cite this

Homogeneous annealing of TiO2, ZrO2 and ITO sol-gel layers with CO2 laser. / Desens, M.; Wesang, K.; Hohnholz, A. et al.
In: Procedia CIRP, Vol. 94, 2020, p. 905-909.

Research output: Contribution to journalConference articleResearchpeer review

Desens, M, Wesang, K, Hohnholz, A, Jäschke, P, Kaierle, S & Overmeyer, L 2020, 'Homogeneous annealing of TiO2, ZrO2 and ITO sol-gel layers with CO2 laser', Procedia CIRP, vol. 94, pp. 905-909. https://doi.org/10.1016/j.procir.2020.09.070
Desens, M., Wesang, K., Hohnholz, A., Jäschke, P., Kaierle, S., & Overmeyer, L. (2020). Homogeneous annealing of TiO2, ZrO2 and ITO sol-gel layers with CO2 laser. Procedia CIRP, 94, 905-909. https://doi.org/10.1016/j.procir.2020.09.070
Desens M, Wesang K, Hohnholz A, Jäschke P, Kaierle S, Overmeyer L. Homogeneous annealing of TiO2, ZrO2 and ITO sol-gel layers with CO2 laser. Procedia CIRP. 2020;94:905-909. Epub 2020 Sept 15. doi: 10.1016/j.procir.2020.09.070
Desens, M. ; Wesang, K. ; Hohnholz, A. et al. / Homogeneous annealing of TiO2, ZrO2 and ITO sol-gel layers with CO2 laser. In: Procedia CIRP. 2020 ; Vol. 94. pp. 905-909.
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title = "Homogeneous annealing of TiO2, ZrO2 and ITO sol-gel layers with CO2 laser",
abstract = "Laser annealed sol-gel layers have the potential to replace the furnace process and expand the field of applications for selective annealed sol-gel coatings. In this study laser annealed TiO2, ZrO2 and ITO layers on glasses are investigated. Processing parameters of the CO2-laser system such as scanning speed, line overlap, laser power and focal spot are evaluated to generate sufficient thermal energy for densification. The ITO annealing process results in a sheet resistance comparable with the furnace annealed samples. Microscope images of the TiO2 and ZrO2 samples show a homogeneous layer morphology. XRD images exhibit crystalline tetragonal ZrO2 as seen in thermally annealed layers.",
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T1 - Homogeneous annealing of TiO2, ZrO2 and ITO sol-gel layers with CO2 laser

AU - Desens, M.

AU - Wesang, K.

AU - Hohnholz, A.

AU - Jäschke, P.

AU - Kaierle, S.

AU - Overmeyer, L.

N1 - Funding Information: The proectj "Laser annealing of coatings for the industrial production" with the acronym "LaSiP" was financed by AIF - IGF 19454 N together with the project partner Fraunhofer Institute for Silicate research (ISC), who prepared the dipcoated samples.

PY - 2020

Y1 - 2020

N2 - Laser annealed sol-gel layers have the potential to replace the furnace process and expand the field of applications for selective annealed sol-gel coatings. In this study laser annealed TiO2, ZrO2 and ITO layers on glasses are investigated. Processing parameters of the CO2-laser system such as scanning speed, line overlap, laser power and focal spot are evaluated to generate sufficient thermal energy for densification. The ITO annealing process results in a sheet resistance comparable with the furnace annealed samples. Microscope images of the TiO2 and ZrO2 samples show a homogeneous layer morphology. XRD images exhibit crystalline tetragonal ZrO2 as seen in thermally annealed layers.

AB - Laser annealed sol-gel layers have the potential to replace the furnace process and expand the field of applications for selective annealed sol-gel coatings. In this study laser annealed TiO2, ZrO2 and ITO layers on glasses are investigated. Processing parameters of the CO2-laser system such as scanning speed, line overlap, laser power and focal spot are evaluated to generate sufficient thermal energy for densification. The ITO annealing process results in a sheet resistance comparable with the furnace annealed samples. Microscope images of the TiO2 and ZrO2 samples show a homogeneous layer morphology. XRD images exhibit crystalline tetragonal ZrO2 as seen in thermally annealed layers.

KW - ITO

KW - Laser annealing sol gel coating

KW - Surface functionalization

KW - TiO2

KW - ZrO2

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DO - 10.1016/j.procir.2020.09.070

M3 - Conference article

AN - SCOPUS:85093364128

VL - 94

SP - 905

EP - 909

JO - Procedia CIRP

JF - Procedia CIRP

SN - 2212-8271

T2 - 11th CIRP Conference on Photonic Technologies, LANE 2020

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