Effects of Cryogenic Treatment on the Microstructure and Mechanical Properties of High-alloyed Tool Steels

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  • Leibniz Institut für Werkstofforientierte Technologien
  • VDEh-Betriebsforschungsinstitut GmbH
  • Voestalpine Deutschland
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Translated title of the contributionEffects of Cryogenic Treatment on the Microstructure and Mechanical Properties of High-alloyed Tool Steels
Original languageMultiple languages
Pages (from-to)287-307
Number of pages21
JournalHTM - Journal of Heat Treatment and Materials
Volume75
Issue number5
Publication statusPublished - 23 Feb 2021

Abstract

In this work, the influence of a cryogenic treatment on the microstructure, mechanical properties and wear resistance of the high-alloyed tool steels X38CrMoV5-3, X153CrMoV12 and ~X190CrVMo20-4 were investigated. Based on tempering curves of the steels, the heat treatment parameters were determined for the mechanical and wear specimens so that the conventionally heat-treated steels and the cryogenically treated steels featured similar hardness. The investigations showed that an almost complete transformation of retained austenite and a more homogeneous distribution of secondary carbides in the microstructure could be achieved by incorporating a cryogenic treatment. However, the cryogenic treatment does not show significantly positive effects on the investigated mechanical properties and wear resistance of the tool steels. The wear resistance of the samples was dominated by primary carbides. The cryogenic treatment would have a positive effect on large tool components with large wall thicknesses in terms of uniform and complete transformation of retained austenite throughout the entire components.

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Effects of Cryogenic Treatment on the Microstructure and Mechanical Properties of High-alloyed Tool Steels. / Schulz, A.; Cui, C.; Steinbacher, M. et al.
In: HTM - Journal of Heat Treatment and Materials, Vol. 75, No. 5, 23.02.2021, p. 287-307.

Research output: Contribution to journalArticleResearchpeer review

Schulz, A, Cui, C, Steinbacher, M, Ümit, T, Wunde, M, Jung, I, Acar, S, Nürnberger, F, Gerstein, G, Herbst, S & Maier, HJ 2021, 'Effects of Cryogenic Treatment on the Microstructure and Mechanical Properties of High-alloyed Tool Steels', HTM - Journal of Heat Treatment and Materials, vol. 75, no. 5, pp. 287-307. https://doi.org/10.3139/105.110422
Schulz, A., Cui, C., Steinbacher, M., Ümit, T., Wunde, M., Jung, I., Acar, S., Nürnberger, F., Gerstein, G., Herbst, S., & Maier, H. J. (2021). Effects of Cryogenic Treatment on the Microstructure and Mechanical Properties of High-alloyed Tool Steels. HTM - Journal of Heat Treatment and Materials, 75(5), 287-307. https://doi.org/10.3139/105.110422
Schulz A, Cui C, Steinbacher M, Ümit T, Wunde M, Jung I et al. Effects of Cryogenic Treatment on the Microstructure and Mechanical Properties of High-alloyed Tool Steels. HTM - Journal of Heat Treatment and Materials. 2021 Feb 23;75(5):287-307. doi: 10.3139/105.110422
Schulz, A. ; Cui, C. ; Steinbacher, M. et al. / Effects of Cryogenic Treatment on the Microstructure and Mechanical Properties of High-alloyed Tool Steels. In: HTM - Journal of Heat Treatment and Materials. 2021 ; Vol. 75, No. 5. pp. 287-307.
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title = "Effects of Cryogenic Treatment on the Microstructure and Mechanical Properties of High-alloyed Tool Steels",
abstract = "In this work, the influence of a cryogenic treatment on the microstructure, mechanical properties and wear resistance of the high-alloyed tool steels X38CrMoV5-3, X153CrMoV12 and ~X190CrVMo20-4 were investigated. Based on tempering curves of the steels, the heat treatment parameters were determined for the mechanical and wear specimens so that the conventionally heat-treated steels and the cryogenically treated steels featured similar hardness. The investigations showed that an almost complete transformation of retained austenite and a more homogeneous distribution of secondary carbides in the microstructure could be achieved by incorporating a cryogenic treatment. However, the cryogenic treatment does not show significantly positive effects on the investigated mechanical properties and wear resistance of the tool steels. The wear resistance of the samples was dominated by primary carbides. The cryogenic treatment would have a positive effect on large tool components with large wall thicknesses in terms of uniform and complete transformation of retained austenite throughout the entire components.",
keywords = "Cryogenic treatment, Mechanical properties, Microstructure, Tool steel, Wear resistance",
author = "A. Schulz and C. Cui and M. Steinbacher and T. {\"U}mit and M. Wunde and I. Jung and S. Acar and F. N{\"u}rnberger and G. Gerstein and S. Herbst and Maier, {H. J.}",
note = "Funding Information: This work was carried out as part of the IGF project 19289 N “Increase of technological properties by cryogenic treatment of tool steels (nanocarbides)” of the FOSTA – Forschungsvereinigung Stahlanwendung e. V., D{\"u}sseldorf, in cooperation with the AWT – Arbeitsgemeinschaft W{\"a}rmebehandlung und Werkstofftechnik e. V., and was founded by the Arbeitsgemeinschaft industrieller Forschungsvereinigungen “Otto-von-Guericke” e. V. (AiF) within the program of Industrial Community Research (IGF) funded by the Federal Ministry of Economics and Energy on the basis of a resolution of the German parliament. We would like to express our appreciation to the project committee for the constructive cooperation and discussion on the research. We would also like to give special thanks to voestalpine High Performance Metals Deutschland GmbH, D{\"o}rrenberg Edelstahl GmbH and Kind & Co for the provision of the tool steels for the study. We are also grateful to Linde AG for providing us with a Cryoflex B80 freezer. ",
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T1 - Effects of Cryogenic Treatment on the Microstructure and Mechanical Properties of High-alloyed Tool Steels

AU - Schulz, A.

AU - Cui, C.

AU - Steinbacher, M.

AU - Ümit, T.

AU - Wunde, M.

AU - Jung, I.

AU - Acar, S.

AU - Nürnberger, F.

AU - Gerstein, G.

AU - Herbst, S.

AU - Maier, H. J.

N1 - Funding Information: This work was carried out as part of the IGF project 19289 N “Increase of technological properties by cryogenic treatment of tool steels (nanocarbides)” of the FOSTA – Forschungsvereinigung Stahlanwendung e. V., Düsseldorf, in cooperation with the AWT – Arbeitsgemeinschaft Wärmebehandlung und Werkstofftechnik e. V., and was founded by the Arbeitsgemeinschaft industrieller Forschungsvereinigungen “Otto-von-Guericke” e. V. (AiF) within the program of Industrial Community Research (IGF) funded by the Federal Ministry of Economics and Energy on the basis of a resolution of the German parliament. We would like to express our appreciation to the project committee for the constructive cooperation and discussion on the research. We would also like to give special thanks to voestalpine High Performance Metals Deutschland GmbH, Dörrenberg Edelstahl GmbH and Kind & Co for the provision of the tool steels for the study. We are also grateful to Linde AG for providing us with a Cryoflex B80 freezer.

PY - 2021/2/23

Y1 - 2021/2/23

N2 - In this work, the influence of a cryogenic treatment on the microstructure, mechanical properties and wear resistance of the high-alloyed tool steels X38CrMoV5-3, X153CrMoV12 and ~X190CrVMo20-4 were investigated. Based on tempering curves of the steels, the heat treatment parameters were determined for the mechanical and wear specimens so that the conventionally heat-treated steels and the cryogenically treated steels featured similar hardness. The investigations showed that an almost complete transformation of retained austenite and a more homogeneous distribution of secondary carbides in the microstructure could be achieved by incorporating a cryogenic treatment. However, the cryogenic treatment does not show significantly positive effects on the investigated mechanical properties and wear resistance of the tool steels. The wear resistance of the samples was dominated by primary carbides. The cryogenic treatment would have a positive effect on large tool components with large wall thicknesses in terms of uniform and complete transformation of retained austenite throughout the entire components.

AB - In this work, the influence of a cryogenic treatment on the microstructure, mechanical properties and wear resistance of the high-alloyed tool steels X38CrMoV5-3, X153CrMoV12 and ~X190CrVMo20-4 were investigated. Based on tempering curves of the steels, the heat treatment parameters were determined for the mechanical and wear specimens so that the conventionally heat-treated steels and the cryogenically treated steels featured similar hardness. The investigations showed that an almost complete transformation of retained austenite and a more homogeneous distribution of secondary carbides in the microstructure could be achieved by incorporating a cryogenic treatment. However, the cryogenic treatment does not show significantly positive effects on the investigated mechanical properties and wear resistance of the tool steels. The wear resistance of the samples was dominated by primary carbides. The cryogenic treatment would have a positive effect on large tool components with large wall thicknesses in terms of uniform and complete transformation of retained austenite throughout the entire components.

KW - Cryogenic treatment

KW - Mechanical properties

KW - Microstructure

KW - Tool steel

KW - Wear resistance

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JO - HTM - Journal of Heat Treatment and Materials

JF - HTM - Journal of Heat Treatment and Materials

SN - 1867-2493

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