Details
| Original language | English |
|---|---|
| Pages (from-to) | 463-474 |
| Number of pages | 12 |
| Journal | Acta Crystallographica Section B: Structural Science, Crystal Engineering and Materials |
| Volume | 75 |
| Publication status | Published - 1 Aug 2019 |
| Externally published | Yes |
Abstract
Electron diffraction tomography (EDT) has gained increasing interest, starting with the development of automated electron diffraction tomography (ADT) which enables the collection of three-dimensional electron diffraction data from nano-sized crystals suitable for ab initio structure analysis. A basic description of the ADT method, nowadays recognized as a reliable and established method, as well as its special features and general applicability to different transmission electron microscopes is provided. In addition, the usability of ADT for crystal structure analysis of single nano-sized crystals with and without special crystallographic features, such as twinning, modulations and disorder is demonstrated.
Keywords
- disorder analysis, electron crystallography, electron diffraction tomography, nanomaterials, single-crystal structure analysis
ASJC Scopus subject areas
- Materials Science(all)
- Electronic, Optical and Magnetic Materials
- Physics and Astronomy(all)
- Atomic and Molecular Physics, and Optics
- Materials Science(all)
- Metals and Alloys
- Materials Science(all)
- Materials Chemistry
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In: Acta Crystallographica Section B: Structural Science, Crystal Engineering and Materials, Vol. 75, 01.08.2019, p. 463-474.
Research output: Contribution to journal › Article › Research › peer review
}
TY - JOUR
T1 - Automated electron diffraction tomography - Development and applications
AU - Kolb, Ute
AU - Krysiak, Yaşar
AU - Plana-Ruiz, Sergi
N1 - Funding information: The following funding is acknowledged: Stipendienstiftung of federal state of Rhineland-Palatinate (grant to Yasar Krysiak); Johannes Gutenberg-Universität Mainz (grant to Yasar Krysiak).
PY - 2019/8/1
Y1 - 2019/8/1
N2 - Electron diffraction tomography (EDT) has gained increasing interest, starting with the development of automated electron diffraction tomography (ADT) which enables the collection of three-dimensional electron diffraction data from nano-sized crystals suitable for ab initio structure analysis. A basic description of the ADT method, nowadays recognized as a reliable and established method, as well as its special features and general applicability to different transmission electron microscopes is provided. In addition, the usability of ADT for crystal structure analysis of single nano-sized crystals with and without special crystallographic features, such as twinning, modulations and disorder is demonstrated.
AB - Electron diffraction tomography (EDT) has gained increasing interest, starting with the development of automated electron diffraction tomography (ADT) which enables the collection of three-dimensional electron diffraction data from nano-sized crystals suitable for ab initio structure analysis. A basic description of the ADT method, nowadays recognized as a reliable and established method, as well as its special features and general applicability to different transmission electron microscopes is provided. In addition, the usability of ADT for crystal structure analysis of single nano-sized crystals with and without special crystallographic features, such as twinning, modulations and disorder is demonstrated.
KW - disorder analysis
KW - electron crystallography
KW - electron diffraction tomography
KW - nanomaterials
KW - single-crystal structure analysis
UR - http://www.scopus.com/inward/record.url?scp=85070601984&partnerID=8YFLogxK
U2 - 10.1107/S2052520619006711
DO - 10.1107/S2052520619006711
M3 - Article
C2 - 32830704
AN - SCOPUS:85070601984
VL - 75
SP - 463
EP - 474
JO - Acta Crystallographica Section B: Structural Science, Crystal Engineering and Materials
JF - Acta Crystallographica Section B: Structural Science, Crystal Engineering and Materials
SN - 2052-5192
ER -