UV-optical and microstructural properties of MgF2-coatings deposited by IBS and PVD processes

Publikation: Beitrag in Buch/Bericht/Sammelwerk/KonferenzbandAufsatz in KonferenzbandForschungPeer-Review

Autoren

  • Detlev Ristau
  • Winfried Arens
  • Salvador Bosch
  • Angela Duparre
  • Enrico Masetti
  • Damien Jacob
  • George Kiriakidis
  • Francesca Peiro
  • Etienne Quesnel
  • Alexander Tikhonravov

Externe Organisationen

  • Universitat de Barcelona (UB)
  • Fraunhofer-Institut für Angewandte Optik und Feinmechanik IOF
  • ENEA-Cassacia
  • Foundation for Research & Technology - Hellas (FORTH)
  • CEA-LETI
  • Lomonosov Moscow State University
  • Laser Zentrum Hannover e.V. (LZH)
Forschungs-netzwerk anzeigen

Details

OriginalspracheEnglisch
Titel des SammelwerksAdvances in Optical Interference Coatings
Untertitel25 - 27 May 1999, Berlin, Germany
ErscheinungsortBellingham
Herausgeber (Verlag)SPIE
Seiten436-445
Seitenumfang10
ISBN (Print)0-8194-3212-1
PublikationsstatusVeröffentlicht - 7 Sept. 1999
Extern publiziertJa
Veranstaltung1999 Advances in Optical Interference Coatings - Berlin, Ger
Dauer: 25 Mai 199927 Mai 1999

Publikationsreihe

NameProceedings of SPIE - The International Society for Optical Engineering
Herausgeber (Verlag)SPIE
Band3738
ISSN (Print)0277-786X

Abstract

In high quality optical coating systems for the DUV-spectral range, MgF2 is one of the preferred deposition materials. MgF2-coatings exhibit relatively low optical losses as well as high stability and laser induced damage thresholds. In the present joint research effort of several European laboratories, the potentiality of MgF2 is evaluated in respect to the production of improved optical coatings for applications in laser technology and semiconductor lithography. For this purpose, single layers of MgF2 were deposited on superpolished fused silica and CaF2-substrates by ion beam sputtering (IBS, [2]), boat (bPVD) and e-beam (ePVD) evaporation in different laboratories. Besides photometric inspections, the samples were characterized by an optical scatter measurement facility at 193 nm and 633 nm. The structural properties were assessed using AFM, XRD, and adapted TEM-techniques involving conventional thinning methods for the layers. For the measurement of mechanical stress in the coatings, special silicon substrates were coated and analyzed. The optical constants of the MgF2-layers, which were determined by two independent data reduction algorithms from the spectral behaviour, are in good agreement with values published in the open literature: The refractive indices range between 1.40 and 1.41 at 248 nm for the PVD and IBS processes. The IBS-process achieves best homogeneity and lowest surface roughness around 1nmrms among the processes compared. In contrast to PVD coatings, which exhibit tensile mechanical stress ranging approximately from 300 to 400 MPa, high compressive stress of up to 910 MPa occurs in the IBS- coatings. The experimental findings are discussed in respect to the microstructural properties and the surface topography of the coatings.

ASJC Scopus Sachgebiete

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UV-optical and microstructural properties of MgF2-coatings deposited by IBS and PVD processes. / Ristau, Detlev; Arens, Winfried; Bosch, Salvador et al.
Advances in Optical Interference Coatings: 25 - 27 May 1999, Berlin, Germany. Bellingham: SPIE, 1999. S. 436-445 (Proceedings of SPIE - The International Society for Optical Engineering; Band 3738).

Publikation: Beitrag in Buch/Bericht/Sammelwerk/KonferenzbandAufsatz in KonferenzbandForschungPeer-Review

Ristau, D, Arens, W, Bosch, S, Duparre, A, Masetti, E, Jacob, D, Kiriakidis, G, Peiro, F, Quesnel, E & Tikhonravov, A 1999, UV-optical and microstructural properties of MgF2-coatings deposited by IBS and PVD processes. in Advances in Optical Interference Coatings: 25 - 27 May 1999, Berlin, Germany. Proceedings of SPIE - The International Society for Optical Engineering, Bd. 3738, SPIE, Bellingham, S. 436-445, 1999 Advances in Optical Interference Coatings, Berlin, Ger, 25 Mai 1999. https://doi.org/10.1117/12.360111
Ristau, D., Arens, W., Bosch, S., Duparre, A., Masetti, E., Jacob, D., Kiriakidis, G., Peiro, F., Quesnel, E., & Tikhonravov, A. (1999). UV-optical and microstructural properties of MgF2-coatings deposited by IBS and PVD processes. In Advances in Optical Interference Coatings: 25 - 27 May 1999, Berlin, Germany (S. 436-445). (Proceedings of SPIE - The International Society for Optical Engineering; Band 3738). SPIE. https://doi.org/10.1117/12.360111
Ristau D, Arens W, Bosch S, Duparre A, Masetti E, Jacob D et al. UV-optical and microstructural properties of MgF2-coatings deposited by IBS and PVD processes. in Advances in Optical Interference Coatings: 25 - 27 May 1999, Berlin, Germany. Bellingham: SPIE. 1999. S. 436-445. (Proceedings of SPIE - The International Society for Optical Engineering). doi: 10.1117/12.360111
Ristau, Detlev ; Arens, Winfried ; Bosch, Salvador et al. / UV-optical and microstructural properties of MgF2-coatings deposited by IBS and PVD processes. Advances in Optical Interference Coatings: 25 - 27 May 1999, Berlin, Germany. Bellingham : SPIE, 1999. S. 436-445 (Proceedings of SPIE - The International Society for Optical Engineering).
Download
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abstract = "In high quality optical coating systems for the DUV-spectral range, MgF2 is one of the preferred deposition materials. MgF2-coatings exhibit relatively low optical losses as well as high stability and laser induced damage thresholds. In the present joint research effort of several European laboratories, the potentiality of MgF2 is evaluated in respect to the production of improved optical coatings for applications in laser technology and semiconductor lithography. For this purpose, single layers of MgF2 were deposited on superpolished fused silica and CaF2-substrates by ion beam sputtering (IBS, [2]), boat (bPVD) and e-beam (ePVD) evaporation in different laboratories. Besides photometric inspections, the samples were characterized by an optical scatter measurement facility at 193 nm and 633 nm. The structural properties were assessed using AFM, XRD, and adapted TEM-techniques involving conventional thinning methods for the layers. For the measurement of mechanical stress in the coatings, special silicon substrates were coated and analyzed. The optical constants of the MgF2-layers, which were determined by two independent data reduction algorithms from the spectral behaviour, are in good agreement with values published in the open literature: The refractive indices range between 1.40 and 1.41 at 248 nm for the PVD and IBS processes. The IBS-process achieves best homogeneity and lowest surface roughness around 1nmrms among the processes compared. In contrast to PVD coatings, which exhibit tensile mechanical stress ranging approximately from 300 to 400 MPa, high compressive stress of up to 910 MPa occurs in the IBS- coatings. The experimental findings are discussed in respect to the microstructural properties and the surface topography of the coatings.",
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AU - Ristau, Detlev

AU - Arens, Winfried

AU - Bosch, Salvador

AU - Duparre, Angela

AU - Masetti, Enrico

AU - Jacob, Damien

AU - Kiriakidis, George

AU - Peiro, Francesca

AU - Quesnel, Etienne

AU - Tikhonravov, Alexander

PY - 1999/9/7

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N2 - In high quality optical coating systems for the DUV-spectral range, MgF2 is one of the preferred deposition materials. MgF2-coatings exhibit relatively low optical losses as well as high stability and laser induced damage thresholds. In the present joint research effort of several European laboratories, the potentiality of MgF2 is evaluated in respect to the production of improved optical coatings for applications in laser technology and semiconductor lithography. For this purpose, single layers of MgF2 were deposited on superpolished fused silica and CaF2-substrates by ion beam sputtering (IBS, [2]), boat (bPVD) and e-beam (ePVD) evaporation in different laboratories. Besides photometric inspections, the samples were characterized by an optical scatter measurement facility at 193 nm and 633 nm. The structural properties were assessed using AFM, XRD, and adapted TEM-techniques involving conventional thinning methods for the layers. For the measurement of mechanical stress in the coatings, special silicon substrates were coated and analyzed. The optical constants of the MgF2-layers, which were determined by two independent data reduction algorithms from the spectral behaviour, are in good agreement with values published in the open literature: The refractive indices range between 1.40 and 1.41 at 248 nm for the PVD and IBS processes. The IBS-process achieves best homogeneity and lowest surface roughness around 1nmrms among the processes compared. In contrast to PVD coatings, which exhibit tensile mechanical stress ranging approximately from 300 to 400 MPa, high compressive stress of up to 910 MPa occurs in the IBS- coatings. The experimental findings are discussed in respect to the microstructural properties and the surface topography of the coatings.

AB - In high quality optical coating systems for the DUV-spectral range, MgF2 is one of the preferred deposition materials. MgF2-coatings exhibit relatively low optical losses as well as high stability and laser induced damage thresholds. In the present joint research effort of several European laboratories, the potentiality of MgF2 is evaluated in respect to the production of improved optical coatings for applications in laser technology and semiconductor lithography. For this purpose, single layers of MgF2 were deposited on superpolished fused silica and CaF2-substrates by ion beam sputtering (IBS, [2]), boat (bPVD) and e-beam (ePVD) evaporation in different laboratories. Besides photometric inspections, the samples were characterized by an optical scatter measurement facility at 193 nm and 633 nm. The structural properties were assessed using AFM, XRD, and adapted TEM-techniques involving conventional thinning methods for the layers. For the measurement of mechanical stress in the coatings, special silicon substrates were coated and analyzed. The optical constants of the MgF2-layers, which were determined by two independent data reduction algorithms from the spectral behaviour, are in good agreement with values published in the open literature: The refractive indices range between 1.40 and 1.41 at 248 nm for the PVD and IBS processes. The IBS-process achieves best homogeneity and lowest surface roughness around 1nmrms among the processes compared. In contrast to PVD coatings, which exhibit tensile mechanical stress ranging approximately from 300 to 400 MPa, high compressive stress of up to 910 MPa occurs in the IBS- coatings. The experimental findings are discussed in respect to the microstructural properties and the surface topography of the coatings.

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