Synthesis and characterization of zeolite A by hydrothermal transformation of natural Jordanian kaolin

Publikation: Beitrag in FachzeitschriftArtikelForschungPeer-Review

Autoren

  • Mousa Gougazeh
  • J. Ch Buhl

Organisationseinheiten

Externe Organisationen

  • Tafila Technical University (TTU)
Forschungs-netzwerk anzeigen

Details

OriginalspracheEnglisch
Seiten (von - bis)35-42
Seitenumfang8
FachzeitschriftJournal of the Association of Arab Universities for Basic and Applied Sciences
Jahrgang15
Ausgabenummer1
Frühes Online-Datum29 Apr. 2013
PublikationsstatusVeröffentlicht - 1 Apr. 2014

Abstract

The synthesis of zeolite materials by hydrothermal transformation of natural Jordanian kaolin in NaOH solutions of various concentrations was investigated at 100. °C for 20. h. A mixture of zeolite A, quartz and hydroxysodalite (HS) was obtained. Zeolite A was the main product with the NaOH concentrations of 1.50-3.50. M, which was confirmed by XRD, IR and SEM. Zeolite A can be obtained from natural kaolin under the conditions applied showing that metakaolinization can be observed at 650. °C which is much lower than the temperatures given in the previous works, 700-950. °C. The products obtained from the experiments were characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM).

Zitieren

Synthesis and characterization of zeolite A by hydrothermal transformation of natural Jordanian kaolin. / Gougazeh, Mousa; Buhl, J. Ch.
in: Journal of the Association of Arab Universities for Basic and Applied Sciences, Jahrgang 15, Nr. 1, 01.04.2014, S. 35-42.

Publikation: Beitrag in FachzeitschriftArtikelForschungPeer-Review

Gougazeh, M & Buhl, JC 2014, 'Synthesis and characterization of zeolite A by hydrothermal transformation of natural Jordanian kaolin', Journal of the Association of Arab Universities for Basic and Applied Sciences, Jg. 15, Nr. 1, S. 35-42. https://doi.org/10.1016/j.jaubas.2013.03.007, https://doi.org/10.15488/666
Gougazeh, M., & Buhl, J. C. (2014). Synthesis and characterization of zeolite A by hydrothermal transformation of natural Jordanian kaolin. Journal of the Association of Arab Universities for Basic and Applied Sciences, 15(1), 35-42. https://doi.org/10.1016/j.jaubas.2013.03.007, https://doi.org/10.15488/666
Gougazeh M, Buhl JC. Synthesis and characterization of zeolite A by hydrothermal transformation of natural Jordanian kaolin. Journal of the Association of Arab Universities for Basic and Applied Sciences. 2014 Apr 1;15(1):35-42. Epub 2013 Apr 29. doi: 10.1016/j.jaubas.2013.03.007, https://doi.org/10.15488/666
Gougazeh, Mousa ; Buhl, J. Ch. / Synthesis and characterization of zeolite A by hydrothermal transformation of natural Jordanian kaolin. in: Journal of the Association of Arab Universities for Basic and Applied Sciences. 2014 ; Jahrgang 15, Nr. 1. S. 35-42.
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title = "Synthesis and characterization of zeolite A by hydrothermal transformation of natural Jordanian kaolin",
abstract = "The synthesis of zeolite materials by hydrothermal transformation of natural Jordanian kaolin in NaOH solutions of various concentrations was investigated at 100. °C for 20. h. A mixture of zeolite A, quartz and hydroxysodalite (HS) was obtained. Zeolite A was the main product with the NaOH concentrations of 1.50-3.50. M, which was confirmed by XRD, IR and SEM. Zeolite A can be obtained from natural kaolin under the conditions applied showing that metakaolinization can be observed at 650. °C which is much lower than the temperatures given in the previous works, 700-950. °C. The products obtained from the experiments were characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM).",
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note = "Funding Information: The authors are grateful to the Tafila Technical University (TTU) and the German Sciences Foundation “Deutsche Forschungsgemeinschaft” (DFG) for financially supporting this study. Special thanks to Prof. C. Ruscher and Dr. Lars Robben for assistance with the acquisition of FTIR, and SEM data, respectively, as well as three anonymous reviewers for constructive comments on the manuscript.",
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AU - Gougazeh, Mousa

AU - Buhl, J. Ch

N1 - Funding Information: The authors are grateful to the Tafila Technical University (TTU) and the German Sciences Foundation “Deutsche Forschungsgemeinschaft” (DFG) for financially supporting this study. Special thanks to Prof. C. Ruscher and Dr. Lars Robben for assistance with the acquisition of FTIR, and SEM data, respectively, as well as three anonymous reviewers for constructive comments on the manuscript.

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N2 - The synthesis of zeolite materials by hydrothermal transformation of natural Jordanian kaolin in NaOH solutions of various concentrations was investigated at 100. °C for 20. h. A mixture of zeolite A, quartz and hydroxysodalite (HS) was obtained. Zeolite A was the main product with the NaOH concentrations of 1.50-3.50. M, which was confirmed by XRD, IR and SEM. Zeolite A can be obtained from natural kaolin under the conditions applied showing that metakaolinization can be observed at 650. °C which is much lower than the temperatures given in the previous works, 700-950. °C. The products obtained from the experiments were characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM).

AB - The synthesis of zeolite materials by hydrothermal transformation of natural Jordanian kaolin in NaOH solutions of various concentrations was investigated at 100. °C for 20. h. A mixture of zeolite A, quartz and hydroxysodalite (HS) was obtained. Zeolite A was the main product with the NaOH concentrations of 1.50-3.50. M, which was confirmed by XRD, IR and SEM. Zeolite A can be obtained from natural kaolin under the conditions applied showing that metakaolinization can be observed at 650. °C which is much lower than the temperatures given in the previous works, 700-950. °C. The products obtained from the experiments were characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM).

KW - Hydrothermal synthesis

KW - Hydroxysodalite

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KW - Metakaolin

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