Silica gel-catalyzed cyclizations of mixed ketene acetals

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OriginalspracheEnglisch
Seiten (von - bis)5241-5244
Seitenumfang4
FachzeitschriftTetrahedron letters
Jahrgang29
Ausgabenummer41
PublikationsstatusVeröffentlicht - 1988

Abstract

Mixed ketene acetals of type 2 undergo smooth cyclization upon treatment with silica gel yielding diastereoselectively bicyclo[2.2.2]octanones of type 3. Alternatively, the same result was obtained by exposure of the substrates to TiCl4 at low temperature.

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Silica gel-catalyzed cyclizations of mixed ketene acetals. / Schinzer, Dieter; Kalesse, Markus; Kabbara, Jazid.
in: Tetrahedron letters, Jahrgang 29, Nr. 41, 1988, S. 5241-5244.

Publikation: Beitrag in FachzeitschriftArtikelForschungPeer-Review

Schinzer D, Kalesse M, Kabbara J. Silica gel-catalyzed cyclizations of mixed ketene acetals. Tetrahedron letters. 1988;29(41):5241-5244. doi: 10.1016/S0040-4039(00)80726-1
Schinzer, Dieter ; Kalesse, Markus ; Kabbara, Jazid. / Silica gel-catalyzed cyclizations of mixed ketene acetals. in: Tetrahedron letters. 1988 ; Jahrgang 29, Nr. 41. S. 5241-5244.
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