Details
Originalsprache | Englisch |
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Titel des Sammelwerks | 2017 30th International Vacuum Nanoelectronics Conference (IVNC) |
Herausgeber/-innen | Christoph Langer, Robert Lawrowski |
Herausgeber (Verlag) | Institute of Electrical and Electronics Engineers Inc. |
Seiten | 102-103 |
Seitenumfang | 2 |
ISBN (elektronisch) | 9781509039753, 978-1-5090-3974-6 |
ISBN (Print) | 978-1-5090-3976-0 |
Publikationsstatus | Veröffentlicht - 2017 |
Veranstaltung | 30th International Vacuum Nanoelectronics Conference - Regensburg, Deutschland Dauer: 10 Juli 2017 → 14 Juli 2017 Konferenznummer: 30 https://www.aconf.org/conf_92671.html |
Publikationsreihe
Name | International Vacuum Nanoelectronics Conference |
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Herausgeber (Verlag) | IEEE |
ISSN (elektronisch) | 2380-6311 |
Abstract
Ion mobility spectrometers (IMS) are measurement devices for fast and ultra-sensitive trace gas analysis. Most IMS employ radioactive electron sources, such as 3H or 63Ni, to provide free electrons with high kinetic energy at atmospheric pressure for initiating a chemical gas phase ionization of the analytes. The disadvantage of these radioactive materials are legal restrictions and the electron emission cannot be adjusted or turned off. Therefore, we developed a non-radioactive electron source and replaced the 3H-source of our existing IMS, leading to comparable spectra. An advantage of our non-radioactive electron source is that it can operate in a fast pulsed mode. By optimizing the geometric parameters and developing fast control electronics, we can achieve short electron emission pulses with high intensities and adjustable pulse width down to a few nanoseconds. This allows to control the ionization process, which can enhance the analytical performance of the IMS. Furthermore, a miniaturized non-radioactive electron source is desirable, e.g. for hand-held IMS devices. Therefore, we developed an emission current control for field emitter cathodes and investigated their suitability for this application.
ASJC Scopus Sachgebiete
- Werkstoffwissenschaften (insg.)
- Elektronische, optische und magnetische Materialien
- Ingenieurwesen (insg.)
- Elektrotechnik und Elektronik
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- BibTex
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2017 30th International Vacuum Nanoelectronics Conference (IVNC). Hrsg. / Christoph Langer; Robert Lawrowski. Institute of Electrical and Electronics Engineers Inc., 2017. S. 102-103 8051563 (International Vacuum Nanoelectronics Conference).
Publikation: Beitrag in Buch/Bericht/Sammelwerk/Konferenzband › Aufsatz in Konferenzband › Forschung › Peer-Review
}
TY - GEN
T1 - Pulsed electron source for atmospheric pressure chemical ionization in ion mobility spectrometry
AU - Bunert, Erik
AU - Heptner, Andre
AU - Kirk, Ansgar T.
AU - Käbein, Oliver
AU - Zimmermann, Stefan
AU - Kusch, Alexander
AU - Wurz, Marc Christopher
N1 - Conference code: 30
PY - 2017
Y1 - 2017
N2 - Ion mobility spectrometers (IMS) are measurement devices for fast and ultra-sensitive trace gas analysis. Most IMS employ radioactive electron sources, such as 3H or 63Ni, to provide free electrons with high kinetic energy at atmospheric pressure for initiating a chemical gas phase ionization of the analytes. The disadvantage of these radioactive materials are legal restrictions and the electron emission cannot be adjusted or turned off. Therefore, we developed a non-radioactive electron source and replaced the 3H-source of our existing IMS, leading to comparable spectra. An advantage of our non-radioactive electron source is that it can operate in a fast pulsed mode. By optimizing the geometric parameters and developing fast control electronics, we can achieve short electron emission pulses with high intensities and adjustable pulse width down to a few nanoseconds. This allows to control the ionization process, which can enhance the analytical performance of the IMS. Furthermore, a miniaturized non-radioactive electron source is desirable, e.g. for hand-held IMS devices. Therefore, we developed an emission current control for field emitter cathodes and investigated their suitability for this application.
AB - Ion mobility spectrometers (IMS) are measurement devices for fast and ultra-sensitive trace gas analysis. Most IMS employ radioactive electron sources, such as 3H or 63Ni, to provide free electrons with high kinetic energy at atmospheric pressure for initiating a chemical gas phase ionization of the analytes. The disadvantage of these radioactive materials are legal restrictions and the electron emission cannot be adjusted or turned off. Therefore, we developed a non-radioactive electron source and replaced the 3H-source of our existing IMS, leading to comparable spectra. An advantage of our non-radioactive electron source is that it can operate in a fast pulsed mode. By optimizing the geometric parameters and developing fast control electronics, we can achieve short electron emission pulses with high intensities and adjustable pulse width down to a few nanoseconds. This allows to control the ionization process, which can enhance the analytical performance of the IMS. Furthermore, a miniaturized non-radioactive electron source is desirable, e.g. for hand-held IMS devices. Therefore, we developed an emission current control for field emitter cathodes and investigated their suitability for this application.
KW - APCI
KW - emission current control
KW - field emission
KW - ion mobility spectrometry
KW - non-radioacitve electron source
KW - pulsed electron emission
KW - thermionic emission
UR - http://www.scopus.com/inward/record.url?scp=85032834764&partnerID=8YFLogxK
U2 - 10.1109/IVNC.2017.8051563
DO - 10.1109/IVNC.2017.8051563
M3 - Conference contribution
AN - SCOPUS:85032834764
SN - 978-1-5090-3976-0
T3 - International Vacuum Nanoelectronics Conference
SP - 102
EP - 103
BT - 2017 30th International Vacuum Nanoelectronics Conference (IVNC)
A2 - Langer, Christoph
A2 - Lawrowski, Robert
PB - Institute of Electrical and Electronics Engineers Inc.
T2 - 30th International Vacuum Nanoelectronics Conference
Y2 - 10 July 2017 through 14 July 2017
ER -