Laboratory X-ray tomography for metal additive manufacturing: Round robin test

Publikation: Beitrag in FachzeitschriftArtikelForschungPeer-Review

Autoren

  • Anton du Plessis
  • Stephan G. du Roux
  • Jess Waller
  • Philip Sperling
  • Nils Achilles
  • Andre Beerlink
  • Francois Métayer
  • Mirko Sinico
  • Gabriel Probst
  • Wim Dewulf
  • Florian Bittner
  • Hans-Josef Endres
  • Marian Willner
  • Agota Drégelyi-Kiss
  • Tomas Zikmund
  • Jakub Laznovsky
  • Jozef Kaiser
  • Pascal Pinter
  • Stefan Dietrich
  • Elena Lopez
  • Oliver Fitzek
  • Porebski Konrad

Externe Organisationen

  • Fraunhofer-Institut für Holzforschung - Wilhelm-Klauditz-Institut (WKI)
  • University of Stellenbosch
  • White Sands Test Facility (WSTF)
  • Volume Graphics GmbH
  • YXLON International GmbH
  • KU Leuven
  • MITOS GmbH
  • Óbuda-Universität
  • Technische Universität Brünn (VRT)
  • Karlsruher Institut für Technologie (KIT)
  • Fraunhofer-Institut für Werkstoff- und Strahltechnik (IWS)
  • Narodowe Centrum Badań Jądrowych (NCBJ)
Forschungs-netzwerk anzeigen

Details

OriginalspracheEnglisch
Aufsatznummer100837
FachzeitschriftAdditive Manufacturing
Jahrgang30
Frühes Online-Datum13 Sept. 2019
PublikationsstatusVeröffentlicht - Dez. 2019
Extern publiziertJa

Abstract

This paper reports on the results of a round robin test conducted by ten X-ray micro computed tomography (micro-CT) laboratories with the same three selected titanium alloy (Ti6Al4V) laser powder bed fusion (L-PBF) test parts. These parts were a 10-mm cube, a 60-mm long and 40-mm high complex-shaped bracket, and a 15-mm diameter rod. Previously developed protocols for micro-CT analysis of these parts were provided to all participants, including suggested scanning parameters and image analysis steps. No further information on the samples were provided, and they were selected from a variety of parts from a previous different type of round robin study where various L-PBF laboratories provided identical parts for micro-CT analysis at one laboratory. In this new micro-CT round robin test which involves various micro-CT laboratories, parts from the previous work were selected such that each part had a different characteristic flaw type, and all laboratories involved in the study analyzed the same set of parts. The 10-mm cube contained subsurface pores just under its top surface (relative to build direction), and all participants could positively identify this. The complex bracket had contour pores around its outer vertical sides, and was warped with two arms deflected towards one another. Both of these features were positively identified by all participants. The 15-mm diameter rod had a layered stop/start flaw, which was also positively identified by all participants. Differences were found among participants for quantitative evaluations, ranging from no quantitative measurement made, to under and overestimation of the values in all analyses attempted. This round robin provides the opportunity to highlight typical causes of errors in micro-CT scanning and image analysis as applied to additively manufactured parts. Some workflow variations, sources of error and ways to increase the reproducibility of such analysis workflows are discussed. The ultimate aim of this work is to advance the efficient use of micro-CT facilities for process optimization and quality inspections for additively manufactured products. The results provide confidence in the use of laboratory micro-CT but also indicate the need for further development of standards, protocols and image analysis workflows for quantitative assessment, especially for direct and quantitative comparisons between different laboratories.

ASJC Scopus Sachgebiete

Zitieren

Laboratory X-ray tomography for metal additive manufacturing: Round robin test. / du Plessis, Anton; du Roux, Stephan G.; Waller, Jess et al.
in: Additive Manufacturing, Jahrgang 30, 100837, 12.2019.

Publikation: Beitrag in FachzeitschriftArtikelForschungPeer-Review

du Plessis, A, du Roux, SG, Waller, J, Sperling, P, Achilles, N, Beerlink, A, Métayer, F, Sinico, M, Probst, G, Dewulf, W, Bittner, F, Endres, H-J, Willner, M, Drégelyi-Kiss, A, Zikmund, T, Laznovsky, J, Kaiser, J, Pinter, P, Dietrich, S, Lopez, E, Fitzek, O & Konrad, P 2019, 'Laboratory X-ray tomography for metal additive manufacturing: Round robin test', Additive Manufacturing, Jg. 30, 100837. https://doi.org/10.1016/j.addma.2019.100837
du Plessis, A., du Roux, S. G., Waller, J., Sperling, P., Achilles, N., Beerlink, A., Métayer, F., Sinico, M., Probst, G., Dewulf, W., Bittner, F., Endres, H.-J., Willner, M., Drégelyi-Kiss, A., Zikmund, T., Laznovsky, J., Kaiser, J., Pinter, P., Dietrich, S., ... Konrad, P. (2019). Laboratory X-ray tomography for metal additive manufacturing: Round robin test. Additive Manufacturing, 30, Artikel 100837. https://doi.org/10.1016/j.addma.2019.100837
du Plessis A, du Roux SG, Waller J, Sperling P, Achilles N, Beerlink A et al. Laboratory X-ray tomography for metal additive manufacturing: Round robin test. Additive Manufacturing. 2019 Dez;30:100837. Epub 2019 Sep 13. doi: 10.1016/j.addma.2019.100837
du Plessis, Anton ; du Roux, Stephan G. ; Waller, Jess et al. / Laboratory X-ray tomography for metal additive manufacturing: Round robin test. in: Additive Manufacturing. 2019 ; Jahrgang 30.
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@article{c5d0a0b8826840e5afaac5aefb8829a5,
title = "Laboratory X-ray tomography for metal additive manufacturing: Round robin test",
abstract = "This paper reports on the results of a round robin test conducted by ten X-ray micro computed tomography (micro-CT) laboratories with the same three selected titanium alloy (Ti6Al4V) laser powder bed fusion (L-PBF) test parts. These parts were a 10-mm cube, a 60-mm long and 40-mm high complex-shaped bracket, and a 15-mm diameter rod. Previously developed protocols for micro-CT analysis of these parts were provided to all participants, including suggested scanning parameters and image analysis steps. No further information on the samples were provided, and they were selected from a variety of parts from a previous different type of round robin study where various L-PBF laboratories provided identical parts for micro-CT analysis at one laboratory. In this new micro-CT round robin test which involves various micro-CT laboratories, parts from the previous work were selected such that each part had a different characteristic flaw type, and all laboratories involved in the study analyzed the same set of parts. The 10-mm cube contained subsurface pores just under its top surface (relative to build direction), and all participants could positively identify this. The complex bracket had contour pores around its outer vertical sides, and was warped with two arms deflected towards one another. Both of these features were positively identified by all participants. The 15-mm diameter rod had a layered stop/start flaw, which was also positively identified by all participants. Differences were found among participants for quantitative evaluations, ranging from no quantitative measurement made, to under and overestimation of the values in all analyses attempted. This round robin provides the opportunity to highlight typical causes of errors in micro-CT scanning and image analysis as applied to additively manufactured parts. Some workflow variations, sources of error and ways to increase the reproducibility of such analysis workflows are discussed. The ultimate aim of this work is to advance the efficient use of micro-CT facilities for process optimization and quality inspections for additively manufactured products. The results provide confidence in the use of laboratory micro-CT but also indicate the need for further development of standards, protocols and image analysis workflows for quantitative assessment, especially for direct and quantitative comparisons between different laboratories.",
keywords = "Additive manufacturing, Flaw detection, Laser powder bed fusion, Non-destructive testing, Seeded flaws, X-ray tomography, microCT",
author = "{du Plessis}, Anton and {du Roux}, {Stephan G.} and Jess Waller and Philip Sperling and Nils Achilles and Andre Beerlink and Francois M{\'e}tayer and Mirko Sinico and Gabriel Probst and Wim Dewulf and Florian Bittner and Hans-Josef Endres and Marian Willner and Agota Dr{\'e}gelyi-Kiss and Tomas Zikmund and Jakub Laznovsky and Jozef Kaiser and Pascal Pinter and Stefan Dietrich and Elena Lopez and Oliver Fitzek and Porebski Konrad",
note = "Funding Information: The South African Department of Science and Technology is acknowledged for support through the Collaborative Program for Additive Manufacturing (CPAM). This research was carried out under the project CEITEC 2020 (LQ1601) with financial support from the Ministry of Education, Youth and Sports of the Czech Republic under the National Sustainability Programme II and support of CEITEC Nano Research Infrastructure (MEYS CR, 2016?2019). Mirko Sinico kindly acknowledges the funding from the H2020-MSCA-ITN-2016 project PAM2 (Precision Additive Metal Manufacturing), EU Framework Programme for Research and Innovation H2020 Grant Agreement No721383. ",
year = "2019",
month = dec,
doi = "10.1016/j.addma.2019.100837",
language = "English",
volume = "30",

}

Download

TY - JOUR

T1 - Laboratory X-ray tomography for metal additive manufacturing: Round robin test

AU - du Plessis, Anton

AU - du Roux, Stephan G.

AU - Waller, Jess

AU - Sperling, Philip

AU - Achilles, Nils

AU - Beerlink, Andre

AU - Métayer, Francois

AU - Sinico, Mirko

AU - Probst, Gabriel

AU - Dewulf, Wim

AU - Bittner, Florian

AU - Endres, Hans-Josef

AU - Willner, Marian

AU - Drégelyi-Kiss, Agota

AU - Zikmund, Tomas

AU - Laznovsky, Jakub

AU - Kaiser, Jozef

AU - Pinter, Pascal

AU - Dietrich, Stefan

AU - Lopez, Elena

AU - Fitzek, Oliver

AU - Konrad, Porebski

N1 - Funding Information: The South African Department of Science and Technology is acknowledged for support through the Collaborative Program for Additive Manufacturing (CPAM). This research was carried out under the project CEITEC 2020 (LQ1601) with financial support from the Ministry of Education, Youth and Sports of the Czech Republic under the National Sustainability Programme II and support of CEITEC Nano Research Infrastructure (MEYS CR, 2016?2019). Mirko Sinico kindly acknowledges the funding from the H2020-MSCA-ITN-2016 project PAM2 (Precision Additive Metal Manufacturing), EU Framework Programme for Research and Innovation H2020 Grant Agreement No721383.

PY - 2019/12

Y1 - 2019/12

N2 - This paper reports on the results of a round robin test conducted by ten X-ray micro computed tomography (micro-CT) laboratories with the same three selected titanium alloy (Ti6Al4V) laser powder bed fusion (L-PBF) test parts. These parts were a 10-mm cube, a 60-mm long and 40-mm high complex-shaped bracket, and a 15-mm diameter rod. Previously developed protocols for micro-CT analysis of these parts were provided to all participants, including suggested scanning parameters and image analysis steps. No further information on the samples were provided, and they were selected from a variety of parts from a previous different type of round robin study where various L-PBF laboratories provided identical parts for micro-CT analysis at one laboratory. In this new micro-CT round robin test which involves various micro-CT laboratories, parts from the previous work were selected such that each part had a different characteristic flaw type, and all laboratories involved in the study analyzed the same set of parts. The 10-mm cube contained subsurface pores just under its top surface (relative to build direction), and all participants could positively identify this. The complex bracket had contour pores around its outer vertical sides, and was warped with two arms deflected towards one another. Both of these features were positively identified by all participants. The 15-mm diameter rod had a layered stop/start flaw, which was also positively identified by all participants. Differences were found among participants for quantitative evaluations, ranging from no quantitative measurement made, to under and overestimation of the values in all analyses attempted. This round robin provides the opportunity to highlight typical causes of errors in micro-CT scanning and image analysis as applied to additively manufactured parts. Some workflow variations, sources of error and ways to increase the reproducibility of such analysis workflows are discussed. The ultimate aim of this work is to advance the efficient use of micro-CT facilities for process optimization and quality inspections for additively manufactured products. The results provide confidence in the use of laboratory micro-CT but also indicate the need for further development of standards, protocols and image analysis workflows for quantitative assessment, especially for direct and quantitative comparisons between different laboratories.

AB - This paper reports on the results of a round robin test conducted by ten X-ray micro computed tomography (micro-CT) laboratories with the same three selected titanium alloy (Ti6Al4V) laser powder bed fusion (L-PBF) test parts. These parts were a 10-mm cube, a 60-mm long and 40-mm high complex-shaped bracket, and a 15-mm diameter rod. Previously developed protocols for micro-CT analysis of these parts were provided to all participants, including suggested scanning parameters and image analysis steps. No further information on the samples were provided, and they were selected from a variety of parts from a previous different type of round robin study where various L-PBF laboratories provided identical parts for micro-CT analysis at one laboratory. In this new micro-CT round robin test which involves various micro-CT laboratories, parts from the previous work were selected such that each part had a different characteristic flaw type, and all laboratories involved in the study analyzed the same set of parts. The 10-mm cube contained subsurface pores just under its top surface (relative to build direction), and all participants could positively identify this. The complex bracket had contour pores around its outer vertical sides, and was warped with two arms deflected towards one another. Both of these features were positively identified by all participants. The 15-mm diameter rod had a layered stop/start flaw, which was also positively identified by all participants. Differences were found among participants for quantitative evaluations, ranging from no quantitative measurement made, to under and overestimation of the values in all analyses attempted. This round robin provides the opportunity to highlight typical causes of errors in micro-CT scanning and image analysis as applied to additively manufactured parts. Some workflow variations, sources of error and ways to increase the reproducibility of such analysis workflows are discussed. The ultimate aim of this work is to advance the efficient use of micro-CT facilities for process optimization and quality inspections for additively manufactured products. The results provide confidence in the use of laboratory micro-CT but also indicate the need for further development of standards, protocols and image analysis workflows for quantitative assessment, especially for direct and quantitative comparisons between different laboratories.

KW - Additive manufacturing

KW - Flaw detection

KW - Laser powder bed fusion

KW - Non-destructive testing

KW - Seeded flaws

KW - X-ray tomography

KW - microCT

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U2 - 10.1016/j.addma.2019.100837

DO - 10.1016/j.addma.2019.100837

M3 - Article

VL - 30

JO - Additive Manufacturing

JF - Additive Manufacturing

M1 - 100837

ER -

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