Details
| Originalsprache | Englisch |
|---|---|
| Seiten (von - bis) | 2134-2140 |
| Seitenumfang | 7 |
| Fachzeitschrift | Advanced Materials |
| Jahrgang | 19 |
| Ausgabenummer | 16 |
| Frühes Online-Datum | 12 Juli 2007 |
| Publikationsstatus | Veröffentlicht - 17 Aug. 2007 |
Abstract
The formation of novel perovskite-type material via an EDTA (ethylenediaminetetraacetic acid)/citric acid complexing method was discussed. The procedure of the EDTA/citric acid complexing synthesis route is usually a low-temperature heating of the sol until gelation, followed by a heat treatment resulting in a pure perovskite powder. The nanometer scale location of the perovskite formation between the intermediates was verified by imaging using transmission electron microscopy (TEM) for ten different conglomerations, with homogeneous results. The inelastic scattered electrons can be resolved energy-dependently, and the resulting energy distribution with its characteristic ionization edges and energy-loss near-edge structures allows conclusions to be drawn about the element itself. TEM and EFTEM provide evidence that the perovskite structure was formed in a nanometer-scale solid-state reaction between the above mentioned intermediates and at their expense.
ASJC Scopus Sachgebiete
- Werkstoffwissenschaften (insg.)
- Ingenieurwesen (insg.)
- Werkstoffmechanik
- Ingenieurwesen (insg.)
- Maschinenbau
Zitieren
- Standard
- Harvard
- Apa
- Vancouver
- BibTex
- RIS
in: Advanced Materials, Jahrgang 19, Nr. 16, 17.08.2007, S. 2134-2140.
Publikation: Beitrag in Fachzeitschrift › Artikel › Forschung › Peer-Review
}
TY - JOUR
T1 - How (Ba0.5Sr0.5)(Fe0.8Zn 0.2)O3-δ and (Ba0.5Sr0.5) (Co0.8Fe0.2)O3-δ perovskites form via an EDTA/citric acid complexing method
AU - Martynczuk, Julia
AU - Arnold, Mirko
AU - Wang, Haihui
AU - Caro, Jürgen
AU - Feldhoff, Armin
PY - 2007/8/17
Y1 - 2007/8/17
N2 - The formation of novel perovskite-type material via an EDTA (ethylenediaminetetraacetic acid)/citric acid complexing method was discussed. The procedure of the EDTA/citric acid complexing synthesis route is usually a low-temperature heating of the sol until gelation, followed by a heat treatment resulting in a pure perovskite powder. The nanometer scale location of the perovskite formation between the intermediates was verified by imaging using transmission electron microscopy (TEM) for ten different conglomerations, with homogeneous results. The inelastic scattered electrons can be resolved energy-dependently, and the resulting energy distribution with its characteristic ionization edges and energy-loss near-edge structures allows conclusions to be drawn about the element itself. TEM and EFTEM provide evidence that the perovskite structure was formed in a nanometer-scale solid-state reaction between the above mentioned intermediates and at their expense.
AB - The formation of novel perovskite-type material via an EDTA (ethylenediaminetetraacetic acid)/citric acid complexing method was discussed. The procedure of the EDTA/citric acid complexing synthesis route is usually a low-temperature heating of the sol until gelation, followed by a heat treatment resulting in a pure perovskite powder. The nanometer scale location of the perovskite formation between the intermediates was verified by imaging using transmission electron microscopy (TEM) for ten different conglomerations, with homogeneous results. The inelastic scattered electrons can be resolved energy-dependently, and the resulting energy distribution with its characteristic ionization edges and energy-loss near-edge structures allows conclusions to be drawn about the element itself. TEM and EFTEM provide evidence that the perovskite structure was formed in a nanometer-scale solid-state reaction between the above mentioned intermediates and at their expense.
UR - http://www.scopus.com/inward/record.url?scp=34548329958&partnerID=8YFLogxK
U2 - 10.1002/adma.200700322
DO - 10.1002/adma.200700322
M3 - Article
AN - SCOPUS:34548329958
VL - 19
SP - 2134
EP - 2140
JO - Advanced Materials
JF - Advanced Materials
SN - 0935-9648
IS - 16
ER -