AFM-based local thermal analysis is a suitable tool to characterize the impact of different grinding techniques on sucrose surface properties

Publikation: Beitrag in FachzeitschriftArtikelForschungPeer-Review

Autorschaft

  • Dana Middendorf
  • Ute Bindrich
  • Petra Mischnick
  • Knut Franke
  • Volker Heinz

Externe Organisationen

  • Deutsches Institut für Lebensmitteltechnik e.V.
  • Technische Universität Braunschweig
Forschungs-netzwerk anzeigen

Details

OriginalspracheEnglisch
Seiten (von - bis)50-58
Seitenumfang9
FachzeitschriftJournal of Food Engineering
Jahrgang235
Frühes Online-Datum21 Apr. 2018
PublikationsstatusVeröffentlicht - Okt. 2018
Extern publiziertJa

Abstract

Influence of roller and ball mill grinding technology applied for sucrose particles in a lipophilic suspension was investigated considering both particle properties and suspension's flow behavior. Especially particle surfaces after grinding were analyzed using a novel approach by combining atomic force microscopy (AFM) and AFM-local thermal analysis (AFM-LTA). This technique is able to characterize local distributions of different surface states on sucrose particles in nano- and microscale by determining local softening temperatures. For the first time, it was possible to demonstrate on molecular level that applied grinding technologies resulted in different surface characteristics with respect to adhesion forces and state of sucrose using AFM-LTA. Differences in flow behavior despite same particle size distributions and solid contents were traced back to the distribution of crystalline and amorphous areas on sucrose particle surfaces.

ASJC Scopus Sachgebiete

Zitieren

AFM-based local thermal analysis is a suitable tool to characterize the impact of different grinding techniques on sucrose surface properties. / Middendorf, Dana; Bindrich, Ute; Mischnick, Petra et al.
in: Journal of Food Engineering, Jahrgang 235, 10.2018, S. 50-58.

Publikation: Beitrag in FachzeitschriftArtikelForschungPeer-Review

Middendorf D, Bindrich U, Mischnick P, Franke K, Heinz V. AFM-based local thermal analysis is a suitable tool to characterize the impact of different grinding techniques on sucrose surface properties. Journal of Food Engineering. 2018 Okt;235:50-58. Epub 2018 Apr 21. doi: 10.1016/j.jfoodeng.2018.04.021
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AU - Middendorf, Dana

AU - Bindrich, Ute

AU - Mischnick, Petra

AU - Franke, Knut

AU - Heinz, Volker

N1 - © 2018 Elsevier Ltd. All rights reserved.

PY - 2018/10

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N2 - Influence of roller and ball mill grinding technology applied for sucrose particles in a lipophilic suspension was investigated considering both particle properties and suspension's flow behavior. Especially particle surfaces after grinding were analyzed using a novel approach by combining atomic force microscopy (AFM) and AFM-local thermal analysis (AFM-LTA). This technique is able to characterize local distributions of different surface states on sucrose particles in nano- and microscale by determining local softening temperatures. For the first time, it was possible to demonstrate on molecular level that applied grinding technologies resulted in different surface characteristics with respect to adhesion forces and state of sucrose using AFM-LTA. Differences in flow behavior despite same particle size distributions and solid contents were traced back to the distribution of crystalline and amorphous areas on sucrose particle surfaces.

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KW - Fat immobilization

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