A Simple and Efficient Process for Large Scale Glycerol Oligomerization by Microwave Irradiation

Publikation: Beitrag in Fachzeitschrift › Artikel › Forschung › Peer-Review

Autoren

  • Rémi Nguyen
  • Nicolas Galy
  • Abhishek K. Singh
  • Florian Paulus
  • Daniel Stöbener
  • Cathleen Schlesener
  • Sunil K. Sharma
  • Rainer Haag
  • Christophe Len

Externe Organisationen

  • University of Delhi
  • Freie Universität Berlin (FU Berlin)
  • Université de Technologie de Compiègne (UTC)
Forschungs-netzwerk anzeigen

Details

OriginalspracheEnglisch
Aufsatznummer123
FachzeitschriftCATALYSTS
Jahrgang7
Ausgabenummer4
PublikationsstatusVeröffentlicht - 19 Apr. 2017
Extern publiziertJa

Abstract

Herein, an optimized method for 100 g scale synthesis of glycerol oligomers using a microwave multimode source and the low priced K2CO3 as catalyst is reported. This method allows the complete conversion of glycerol to its oligomers in only 30 min, yielding molecular weights up to 1000 g mol−1. Furthermore, a simple iterative purification process, involving the precipitation of the crude product in acetone and methanol, affords a final product composed of larger oligomers with a narrow dispersity (D < 1.5).

ASJC Scopus Sachgebiete

Zitieren

A Simple and Efficient Process for Large Scale Glycerol Oligomerization by Microwave Irradiation. / Nguyen, Rémi; Galy, Nicolas; Singh, Abhishek K. et al.
in: CATALYSTS, Jahrgang 7, Nr. 4, 123, 19.04.2017.

Publikation: Beitrag in Fachzeitschrift › Artikel › Forschung › Peer-Review

Nguyen, R, Galy, N, Singh, AK, Paulus, F, Stöbener, D, Schlesener, C, Sharma, SK, Haag, R & Len, C 2017, 'A Simple and Efficient Process for Large Scale Glycerol Oligomerization by Microwave Irradiation', CATALYSTS, Jg. 7, Nr. 4, 123. https://doi.org/10.3390/catal7040123
Nguyen, R., Galy, N., Singh, A. K., Paulus, F., Stöbener, D., Schlesener, C., Sharma, S. K., Haag, R., & Len, C. (2017). A Simple and Efficient Process for Large Scale Glycerol Oligomerization by Microwave Irradiation. CATALYSTS, 7(4), Artikel 123. https://doi.org/10.3390/catal7040123
Nguyen R, Galy N, Singh AK, Paulus F, Stöbener D, Schlesener C et al. A Simple and Efficient Process for Large Scale Glycerol Oligomerization by Microwave Irradiation. CATALYSTS. 2017 Apr 19;7(4):123. doi: 10.3390/catal7040123
Nguyen, Rémi ; Galy, Nicolas ; Singh, Abhishek K. et al. / A Simple and Efficient Process for Large Scale Glycerol Oligomerization by Microwave Irradiation. in: CATALYSTS. 2017 ; Jahrgang 7, Nr. 4.
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T1 - A Simple and Efficient Process for Large Scale Glycerol Oligomerization by Microwave Irradiation

AU - Nguyen, Rémi

AU - Galy, Nicolas

AU - Singh, Abhishek K.

AU - Paulus, Florian

AU - Stöbener, Daniel

AU - Schlesener, Cathleen

AU - Sharma, Sunil K.

AU - Haag, Rainer

AU - Len, Christophe

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KW - Glycerol

KW - Microwave

KW - Oligomerization

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